发明名称 |
Dry process for producing diborane |
摘要 |
Diborane is produced by reacting lithium or sodium borohydride with boron trifluoride in the absence of a solvent, thereby avoiding the dangers associated with the ether solvents previously used in similar reactions. The reaction appears to proceed via hydride abstraction from the borohydride, rather than via the hydride-halide exchange mechanism in the corresponding reaction in ether solution. Yields of about 95% can be achieved.
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申请公布号 |
US4388284(A) |
申请公布日期 |
1983.06.14 |
申请号 |
US19810303387 |
申请日期 |
1981.09.18 |
申请人 |
THE OHIO STATE UNIVERSITY RESEARCH FOUNDATION |
发明人 |
SHORE, SHELDON G.;TOFT, MARK A. |
分类号 |
C01B6/10;(IPC1-7):C01B6/10 |
主分类号 |
C01B6/10 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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