摘要 |
The phosphide of aluminium or magnesium is produced by reacting the finely divided metal or an alloy of the two metals with yellow phosphorus at a temperature from 300 to 600 DEG C in an inert gas atmosphere and in the presence of a catalytically effective amount of water, the element chlorine, bromine, or iodine or a compound of such element with phosphorus, sulphur, hydrogen, ammonium, zinc, or the metal being reacted. Both the yellow phosphorus in liquid form and the finely divided metal are slowly fed into the reaction vessel. |