发明名称 Process for preparing a mixture which is suitable for perfumery purposes
摘要 A mixture which contains the compound of the formula (1) given in Patent Claim 1 as the main component is prepared while thoroughly mixing acrolein (7) with myrcenol (5); the reaction is carried out (1) in the presence of a catalytic quantity of a Lewis acid catalyst, specifically any one of the following: ZnCl2, SnCl4, ZnBr2, aluminium chloride or C2H5AlCl2, or of a mixture of two or more of these Lewis acids, (2) at a temperature in the range from -20 DEG C up to 100 DEG C, and (3) under a pressure of 1-100 atm., where the molar ratio of acrolein reaction components:myrcenol reaction component is in the range from 10:1 to 1:10 and the quantity of Lewis acid catalyst in per cent by weight, based on the total weight of acrolein and myrcenol, is 0.2 to 10%. The mixture can be used as a component of perfumes or of perfumed articles.
申请公布号 CH632671(A5) 申请公布日期 1982.10.29
申请号 CH19810004067 申请日期 1981.06.19
申请人 INTERNATIONAL FLAVORS & FRAGRANCES INC. 发明人 JAMES MILTON SANDERS;WILLIAM I. TAYLOR;IRA D. HILL;JOHN J. KRYSCHUK;WILLIAM L. SCHREIBER;JOHN B. HALL
分类号 C07C45/64;A61K8/33;A61Q13/00;B01J27/00;B01J31/00;C07C45/00;C07C45/69;C07C47/38;C07C47/42;C07C47/46;C07C67/00;C07C69/02;C07C401/00;C07C403/02;C07C403/04;C07C403/08;C07C403/12;C11B9/00;(IPC1-7):A61K7/46 主分类号 C07C45/64
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