发明名称 Process for the preparation of azidobenzal compounds
摘要 A process for preparing a 2,6-bis-[(4-azidophenyl)methylene]-cyclohexanone of the formula <IMAGE> wherein R is hydrogen or alkyl of 1-6 C atoms, comprises condensing a cyclohexanone of the formula <IMAGE> wherein R is as defined above, with 4-aminobenzaldehyde, the 4-amino group optionally being protected, in the presence of an alkaline condensing agent; removing the protective group when the 4-amino group is protected; diazotizing the resultant 2,6-bis-[(4-aminophenyl)methylene]-cyclohexanone of the formula <IMAGE> wherein R is as defined above, and reacting the diazotization product with an alkali metal azide.
申请公布号 US4354976(A) 申请公布日期 1982.10.19
申请号 US19800218250 申请日期 1980.12.19
申请人 MERCK PATENT GESELLSCHAFT MIT BESCHRAENKTER HAFTUNG 发明人 ROEMER, MICHAEL
分类号 C07C247/16;C07C67/00;C07C241/00;C08K5/22;C09D115/00;(IPC1-7):C07C117/00 主分类号 C07C247/16
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