发明名称 Catalyst for and method of preparing cellulose esters
摘要 Disclosed is a catalyst and a method of preparing lower fatty acid esters of cellulose which comprises esterifying at a temperature of between about 75 DEG C. and about 110 DEG C. a cellulose compound having esterifiable hydroxyl groups with an esterifying bath comprising an organic acid anhydride, a diluent, and a catalyst comprising (a) from about 0.3 to about 3.0% by weight, based on the weight of cellulose, of an acid selected from the group consisting of sulfuric acid, p-toluene sulfonic acid, methane sulfonic acid, methane disulfonic acid and m-benzene disulfonic acid, and (b) from about 0.05 to about 0.3% by weight, based on the weight of cellulose, of a dialkyl phosphite, the alkyl groups of which contain from 2 to 4 carbon atoms, the weight ratio of said bath to the cellulose being between about 5:1 and about 10:1.
申请公布号 US4329447(A) 申请公布日期 1982.05.11
申请号 US19800182521 申请日期 1980.08.29
申请人 EASTMAN KODAK COMPANY 发明人 BREWER, RICHARD J.;WININGER, BRICE S.
分类号 C08B3/02;C08B3/06;(IPC1-7):C08B3/06 主分类号 C08B3/02
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