发明名称 PREPARATION PROCESS OF 2-CHLORO PYRIMIDINE
摘要 <p>Preparation process of 2-chloro pyrimidine from 2-amino pyrimidine, hydrochloric acid and an alkali metal nitrite, the reagents being in substantially similar proportions as in the previously known methods, consisting in preparing a mixture of hydrochloric acid and of a non-polar solvent of low boiling point, then adding 2-amino pyrimidine wherein there is slowly added, at room temperature, the chloride of a metal selected from the group consisting of the titanium, iron, copper and zinc, then introduced, under an inert gas circulation, the selected nitrite at a temperature not exceeding 10.degree.C and finally poured the reaction mixture in iced water.</p>
申请公布号 CA1097640(A) 申请公布日期 1981.03.17
申请号 CA19790328725 申请日期 1979.05.30
申请人 EXPANSIA 发明人 DEMOSTHENE, CLAUDE G.;ASPISI, CHRISTIAN R.
分类号 B01J27/00;C07D239/30;(IPC1-7):07D239/30 主分类号 B01J27/00
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