发明名称 |
Process for the preparation of at least partially sulfonated naphthalene, and use of this product in the purification of naphthalene. |
摘要 |
1. Process for the preparation of at least partially sulphonated naphthalene by the reaction of sulphuric acid with naphthalene, in the presence of a solvent forming an azeotrope with water, characterised in that the molar ratio sulphuric acid/naphthalene is less than 1 and in that the reaction of the sulphuric acid on the naphthalene is carried out between 90 and 150 degrees C thus totally eliminating water in a continuous manner from the reaction medium by azeotropic distillation by means of a solvent chosen from saturated aliphatic hydrocarbons, saturated cycloaliphatic hydrocarbons or their mixtures so that the product obtained is completely free from water and sulphuric acid.
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申请公布号 |
EP0015831(A1) |
申请公布日期 |
1980.09.17 |
申请号 |
EP19800400278 |
申请日期 |
1980.02.29 |
申请人 |
SOCIETE CHIMIQUE DES CHARBONNAGES |
发明人 |
CALIN, PAUL |
分类号 |
C07C7/00;C07C7/148;C07C309/35;C07C317/14;(IPC1-7):C07C7/00;C07C7/14;C07C15/24;C07C147/06 |
主分类号 |
C07C7/00 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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