发明名称 Preparation of hexanitrostilbene
摘要 There is disclosed a process for converting 2,2', 4,4', 6,6'-hexanitrobibenzyl (HNBB) to 2,2', 4,4', 6,6'-hexanitrostilbene (HNS) in high yields by reacting HNBB with a halogenating agent in the presence of a base in an organic solvent or a liquid suspending agent. A preferred halogenating agent is bromine; a preferred base is pyridine; a preferred solvent is dimethylformamide; and a preferred liquid suspending agent is toluene or chlorobenzene.
申请公布号 US4221746(A) 申请公布日期 1980.09.09
申请号 US19790020889 申请日期 1979.03.15
申请人 THE UNITED STATES OF AMERICA AS REPRESENTED BY THE SECRETARY OF THE ARMY 发明人 GILBERT, EVERETT E.
分类号 C07C205/06;(IPC1-7):C07C79/10 主分类号 C07C205/06
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