发明名称 Manufacture of a highly concentrated aqueous solution of a dicarboxylic acid diamine salt and a nylon precondensate
摘要 A process for the manufacture of a highly concentrated aqueous solution of a salt of a dicarboxylic acid and a diamine, as well as of a nylon precondensate, by reacting an alkanedicarboxylic acid of 6 to 12 carbon atoms and a diamine of the formula NH2RNH2, where R is alkylene of 6 to 12 carbon atoms or is <IMAGE> <IMAGE> An aqueous solution, of lower concentration, of a salt of a dicarboxylic acid and a diamine, containing an appropriate dissolved excess of the particular dicarboxylic acid, is reacted with the particular diamine in the molten state, in an equivalent amount to the dissolved dicarboxylic acid, the reaction being carried out under superatmospheric pressure and the final reaction temperature being kept at from 140 DEG to 210 DEG C. The solution obtained is used for the manufacture of a nylon.
申请公布号 US4213884(A) 申请公布日期 1980.07.22
申请号 US19780913641 申请日期 1978.06.08
申请人 BASF AG 发明人 ECKELL, ALBRECHT;MATTHIES, PAUL;PILZ, GEORG;ROTZOLL, RUDI-HEINZ
分类号 C07C55/02;C07C51/00;C07C51/41;C07C67/00;C07C209/00;C07C211/09;C07C211/36;C07C231/00;C07C231/02;C07C231/24;C07C233/36;C07C233/41;(IPC1-7):C08G69/28;C07C51/52 主分类号 C07C55/02
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