发明名称 Process for producing 4,4{40 -dihydroxydiphenylsulfone of high purity
摘要 In a process for producing 4,4'-dihydroxydiphenylsulfone by reacting phenol with sulfuric acid in the presence of a solvent, an improvement which comprises using at least a member selected from the group consisting of chlorobenzene, dichlorobenzene, trichlorobenzene, chlorotoluene, diethylbenzene, xylene, decalin, tetralin and tetrachloroethane as the solvent and removing said solvent progressively and finally substantially completely from the mixture while maintaining the reaction mixture at a temperature of about 160 DEG to about 200 DEG C. to effect precipitation of 4,4'-dihydroxydiphenylsulfone and isomerization of 2,4'-dihydroxydiphenylsulfone to 4,4'-dihydroxydiphenylsulfone.
申请公布号 US4162270(A) 申请公布日期 1979.07.24
申请号 US19780896611 申请日期 1978.04.14
申请人 KONISHI CHEMICAL INDUSTRIES CO LTD 发明人 NAKAGAKI, SHOJI;OGATA, EIJI;ONO, KOJI
分类号 C07C315/00;C07C317/22;(IPC1-7):C07C147/10 主分类号 C07C315/00
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