发明名称 High vacuum freeze-drying
摘要 Water-soluble, substantially anhydrous materials such as anhydrous aspirin salt and anhydrous calcium aspirin salt, stable to hydrolysis, are prepared by subjecting a freeze-dried water-soluble material containing molecularly bound water which is susceptible to hydrolysis to a vacuum of 10 microns or less Hg to remove the molecularly bound water and condensing the removed water on a condenser below -50 DEG C.
申请公布号 US4117603(A) 申请公布日期 1978.10.03
申请号 US19760755000 申请日期 1976.12.28
申请人 SMITH, WALTON J. 发明人 SMITH, WALTON J.
分类号 C07C65/10;F26B5/06;(IPC1-7):F26B5/06 主分类号 C07C65/10
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