发明名称 |
Process for producing mixture containing 4-(4{40 -methyl-4{40 -hydroxyamyl)-{66 {hu 3{b -cyclohexene carboxaldehyde |
摘要 |
A process is described for reacting "myrac aldehyde" having the structure: <IMAGE> (which structure is representative of a mixture of two compounds, one where the carboxaldehyde is in the "4" position and the other wherein the carboxaldehyde is in the "5" position) with an acid hydrating agent at a temperature of from 0 DEG up to 120 DEG C, to produce a mixture containing a major proportion of 4-(4'-methyl-4'-hydroxyamyl)- DELTA 3-cyclohexene carboxaldehyde and a minor proportion of 3-(4'-methyl-4'-hydroxyamyl)- DELTA 3-cyclohexene carboxaldehyde (otherwise termed "Lyral") having the structure: <IMAGE> and a minor proportion of 3-(4'-methyl-4'-hydroxyamyl)- DELTA 3-cyclohexene carboxaldehyde having the structure: <IMAGE> which mixture possesses a sweet, lilac-lily aromatic odor and isolating a mixture of the two carboxaldehydes. The products produced by the aforementioned process are useful in various aspects of perfumery.
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申请公布号 |
US4031161(A) |
申请公布日期 |
1977.06.21 |
申请号 |
US19760694391 |
申请日期 |
1976.06.09 |
申请人 |
INTERNATIONAL FLAVORS & FRAGRANCES INC. |
发明人 |
SANDERS, JAMES MILTON;TAYLOR, WILLIAM I.;HILL, IRA D.;KRYSCHUK, JOHN J. |
分类号 |
C07C45/69;C07C47/46;C11B9/00;(IPC1-7):C07C45/00 |
主分类号 |
C07C45/69 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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