发明名称 Continuous process for concurrent production of dinitrotoluene and high-strength nitric acid
摘要 Dinitrotoluene and nitric acid are concurrently produced by continuously introducing toluene, nitrogen dioxide and oxygen in a molar ratio of at least 4 mols nitrogen dioxide and 1 mol oxygen per mol toluene into a reaction zone containing a reaction medium comprising dinitrotoluene and 93-103% nitric acid, maintaining the resulting mixture of toluene, nitrogen dioxide, oxygen and reaction medium under a pressure of at least 100 psig and at a temperature up to about 100 DEG C. until a reaction product containing dinitrotoluene and 93-103% nitric acid in the ratio of about 1 mol dinitrobenzene and 2 mols nitric acid is produced, and continuously removing said reaction product from the reaction zone.
申请公布号 US4028425(A) 申请公布日期 1977.06.07
申请号 US19760691912 申请日期 1976.06.01
申请人 THE UNITED STATES OF AMERICA AS REPRESENTED BY THE SECRETARY OF THE ARMY 发明人 GILBERT, EVERETT E.
分类号 C01B21/38;C07C205/06;(IPC1-7):C07C79/10 主分类号 C01B21/38
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