发明名称 PREPARATION OF SILICA GELS
摘要 Silica xerogels having a narrow pore diameter distribution in the range of 300-600 A. and surface areas in the range from 200-500 m.2/g. and the process of preparing such xerogels comprising critically controlled steps of precipitation of the silica gel, heat aging the precipitated silica hydrogel slurry, washing the aged product with solutions of salts having displacing effect on sodium, disintegrating the gel, drying the gel by azeotropic distillation with a solvent which is nonmiscible with water, and calcining. Also, a process for preparing such xerogels wherein the non-water miscible solvent is continuously recycled so that a minimum amount of solvent need be used.
申请公布号 US3652216(A) 申请公布日期 1972.03.28
申请号 USD3652216 申请日期 1968.10.11
申请人 NATIONAL PETRO CHEMICALS CO. INC. 发明人 JEROME H. KREKELER;HENRI A. ABOUTBOUL;WILLIAM KIRCH
分类号 B01J20/10;B01J21/08;B01J35/10;C01B33/113;C01B33/154;C01B33/16;C08F10/02;(IPC1-7):C01B33/16 主分类号 B01J20/10
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