摘要 |
1,157,032. Bis - (4 - aminophenyl) methane. MOBAY CHEMICAL CO. 3 Aug., 1967 [5 Aug., 1966], No. 35743/67. Heading C2C. A diaminodiphenylmethane containing at least 96% of the title isomer is prepared by reacting 1 mole CH 2 O with 1À4-6 moles PhNH 2 in presence of 30-100% of the acid required to react with all of the latter, the acid being also sufficient to give a single reaction phase, by conducting the PhNH 2 +acid continuously through a conduit and injecting CH 2 O into the flowing stream at at least 3 points along the conduit. |