发明名称 METHOD FOR PRODUCING ALKYL CELLULOSE
摘要 Provided is a method for producing an alkyl cellulose having a high viscosity and not having an excessively high gel strength. More specifically, there is provided a method for producing an alkyl cellulose comprising the steps of: mixing a cellulose pulp with a first alkali metal hydroxide solution with stirring to obtain alkali cellulose; reacting the alkali cellulose with an alkylating agent to obtain a first reaction mixture; blending a second alkali metal hydroxide solution with the first reaction mixture with stirring, without further blending of the alkylating agent, to obtain a second reaction mixture; and purifying the second reaction mixture to obtain an alkyl cellulose. There is also provided an alkyl cellulose being produced by the above method and having a degree of substitution of alkyl group of 27 to 33% by weight.
申请公布号 US2016168271(A1) 申请公布日期 2016.06.16
申请号 US201514965149 申请日期 2015.12.10
申请人 Shin-Etsu Chemical Co., Ltd. ;SE Tylose GmbH & Co. KG 发明人 Kitamura Akira;Yamamoto Atsushi;Narita Mitsuo;Nebel Heiko;Schultz Andreas
分类号 C08B11/02 主分类号 C08B11/02
代理机构 代理人
主权项 1. A method for producing an alkyl cellulose, comprising the steps of: mixing a cellulose pulp with a first alkali metal hydroxide solution with stirring to obtain alkali cellulose; reacting the alkali cellulose with an alkylating agent to obtain a first reaction mixture; blending a second alkali metal hydroxide solution with the first reaction mixture with stirring, without further blending of the alkylating agent, to obtain a second reaction mixture; and purifying the second reaction mixture to obtain the alkyl cellulose, wherein a ratio of a weight of a first alkali metal hydroxide in the first alkali metal hydroxide solution to a total weight of the first alkali metal hydroxide and a second alkali metal hydroxide in the second alkali metal hydroxide solution is 50 to 86%.
地址 Tokyo JP