发明名称 |
Method for preparing a masterbatch of natural rubber and magnesium-doped silica |
摘要 |
Method for preparing a silica/natural rubber masterbatch, including: doping the silica with magnesium; preparing at least one dispersion of the resulting doped silica in water; bringing a natural rubber field latex into contact with the aqueous doped-silica dispersion and mixing them together so as to obtain a coagulum; recovering the coagulum; and drying the recovered coagulum so as to obtain the masterbatch. |
申请公布号 |
US9505890(B2) |
申请公布日期 |
2016.11.29 |
申请号 |
US201214350440 |
申请日期 |
2012.10.10 |
申请人 |
COMPAGNIE GENERALE DES ETABLISSEMENTS MICHELIN;MICHELIN RECHERCHE ET TECHNIQUE, S.A. |
发明人 |
De Gaudemaris Benoit;Laffargue Geraldine;Berriot Julien |
分类号 |
C08J3/22;C08K9/02;C08J3/215;C08K3/36;C08J3/205;B60C1/00 |
主分类号 |
C08J3/22 |
代理机构 |
Dickinson Wright PLLC |
代理人 |
Dickinson Wright PLLC |
主权项 |
1. A method for preparing a masterbatch of silica/natural rubber comprising:
doping a silica with magnesium thereby obtaining a doped silica, wherein the level of magnesium doping in the silica is from 0.4 to 0.9% by weight per 100 parts by weight of silica; preparing at least one dispersion of the resulting doped silica in water; bringing a concentrated natural rubber latex into contact with the aqueous doped-silica dispersion, wherein the concentrated natural rubber latex and the aqueous doped-silica dispersion have a formulation pH upon contact with one another of greater than or equal to 8.5; mixing the concentrated natural rubber latex and the aqueous doped-silica dispersion together, thereby obtaining a coagulum; recovering the coagulum; and drying the recovered coagulum, thereby obtaining the masterbatch. |
地址 |
Clermont-Ferrand FR |