发明名称 |
PROCESSES FOR PRODUCING ADIPIC ACID FROM FERMENTATION BROTHS CONTAINING DIAMMONIUM ADIPATE |
摘要 |
Processes for making AA from either a clarified DAA-containing fermentation broth or a clarified MAA-containing fermentation broth that include distilling the broth under super atmospheric pressure at a temperature of > 100°C to about 300°C to form an overhead that comprises water and ammonia, and a liquid bottoms that includes AA, and at least about 20 wt% water; cooling the bottoms to a temperature sufficient to cause the bottoms to separate into a liquid portion and a solid portion that is substantially pure AA; and separating the solid portion from the liquid portion. A method also reduces the broth distillation temperature and pressure by adding an ammonia separating and/or water azeotroping solvent to the broth.
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申请公布号 |
CA2738164(A1) |
申请公布日期 |
2011.10.30 |
申请号 |
CA20112738164 |
申请日期 |
2011.04.21 |
申请人 |
BIOAMBER S.A.S. |
发明人 |
FRUCHEY, OLAN S.;MANZER, LEO E.;DUNUWILA, DILUM;KEEN, BRIAN T.;ALBIN, BROOKE A.;CLINTON, NYE A.;DOMBEK, BERNARD D. |
分类号 |
C07C51/43;C07C51/02;C07C55/14;C12P7/44;C12P13/00 |
主分类号 |
C07C51/43 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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