发明名称 PRODUCTION METHOD FOR POLYTHIOL COMPOUND, POLYMERIZABLE COMPOSITION FOR OPTICAL MATERIAL AND USE THEREFOR
摘要 Provided is a method for producing a polythiol compound, comprising: a step for reacting a polyalcohol compound represented by the following formula (4) with thiourea in the presence of hydrogen chloride to obtain an isothiuronium salt; a step for adding, while maintaining a reaction solution containing the isothiuronium salt thus obtained at a temperature of 20°C to 60°C, aqueous ammonia to the reaction solution within 80 minutes, thereby hydrolyzing the isothiuronium salt to obtain a polythiol compound containing, as a main component, one kind or two or more kinds selected from the group consisting of compounds represented by the following formulae (6) to (8); and a step for adding hydrochloric acid which is a concentration of 30% to 36% to the solution containing the polythiol compound thus obtained, washing the solution at a temperature of 30°C to 55°C to purify the polythiol compound.
申请公布号 EP2845847(B1) 申请公布日期 2016.08.31
申请号 EP20130879273 申请日期 2013.02.28
申请人 MITSUI CHEMICALS, INC. 发明人 KAWAGUCHI, MASARU;NISHIMURA, TAKESHI
分类号 C07C319/20;C07C321/14;C08G18/38;C08G75/00;G02B1/04 主分类号 C07C319/20
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