发明名称 |
Process for the continuous manufacture of cellulose glycolate |
摘要 |
In the manufacture of cellulose glycolate, a reaction mixture comprising per 1 part by weight of cellulose 0.2 to 0.6 part by weight of sodium hydroxide, 0.5 to 1.75 parts by weight of sodium monochloroacetate, 7 to 22 parts by weight of isopropanol, and from 20% to 50% by weight, based on the weight of isopropanol, of water is subjected to shearing forces at a temperature less than 30 DEG C to effect intimate mixing and then reacted to cause etherification of the cellulose in a reaction area held at a temperature in the range of 60 DEG C to 90 DEG C and held constant within each section of the reaction area. The residence time of the mixture in the mixing zone is at most one-tenth of its residence time in the reaction area. The solid and liquid components of the reaction mixture after etherification are separated mechanically.
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申请公布号 |
US4017671(A) |
申请公布日期 |
1977.04.12 |
申请号 |
US19750539035 |
申请日期 |
1975.01.06 |
申请人 |
HOECHST AKTIENGESELLSCHAFT |
发明人 |
SCHMINKE, WOLFGANG;STOLTING, KLAUS;MACHOLDT, HANS;KUNKLER, HANS |
分类号 |
C08B11/12;C08B17/00;(IPC1-7):C08B11/00 |
主分类号 |
C08B11/12 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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