METHODS FOR PRODUCING GRAPHENE WITH TUNABLE PROPERTIES BY A MULTI-STEP THERMAL REDUCTION PROCESS
摘要
The present invention refers to process for the preparation of graphene which comprises the steps of a) flash thermal treatment of a graphite oxide at a temperature up to 700°C sufficient to produce exfoliation and under inert atmosphere; b) cooling the material obtained in the previous step below 90°C and c) heating the material resulting from the previous step under inert atmosphere at a temperature which is higher than the temperature of step a), wherein the heating rate is between 1 and 15°C/min. The invention is also directed to the graphenes so obtained, which show excellent physico-chemical properties.
申请公布号
EP3148933(A1)
申请公布日期
2017.04.05
申请号
EP20150763371
申请日期
2015.09.17
申请人
Repsol, S.A.
发明人
PÁEZ DUEÑAS, Antonio;GARCÍA SAN LUIS, Jesús;ÁLVAREZ RODRÍGUEZ, Patricia;GRANDA, Marcos;BLANCO RODRÍGUEZ, Clara;SANTAMARÍA RAMÍREZ, Ricardo;BLANCO, Patricia;FERNÁNDEZ, Laura;MENÉNDEZ LÓPEZ, Rosa María;CALLE GÓMEZ, Fernando