发明名称 anti−アントラジカルコゲノフェンの合成方法
摘要 A method for synthesizing anti-anthradichalcogenophene comprises: a step of reacting a compound represented by formula (1) with a halogenating agent to produce a compound represented by formula (2); a step of reacting the compound represented by formula (2) with a dealkylating agent to produce a compound represented by formula (3); a step of reacting the compound represented by formula (3) with an acetylating agent to produce a compound represented by formula (4); a step of reacting the compound represented by formula (4) with a terminal-acethylene compound to produce a compound represented by formula (5); and a step of reacting the compound represented by formula (5) with a base to cause the cyclization of the compound, thereby producing a compound represented by formula (6). In the formulae, R1 represents an alkyl group; X represents a halogen atom; Ac represents an acetyl group; R2 represents a trimethylsilyl group, a phenyl group or an alkyl group; and R3 represents a hydrogen atom, a phenyl group or an alkyl group.
申请公布号 JP5888815(B2) 申请公布日期 2016.03.22
申请号 JP20120177435 申请日期 2012.08.09
申请人 日本化薬株式会社 发明人 瀧宮 和男
分类号 C07D495/04;C07D517/04 主分类号 C07D495/04
代理机构 代理人
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