发明名称 PROCEDE DE FABRICATION D'AEROGELS PAR CHAUFFAGE DIELECTRIQUE
摘要 The present invention relates to a process for producing aerogels, comprising the following successive steps: a) formation or casting of a sol in a reactor, optionally in the presence of a reinforcing material and/or an additive, b) complete gelling of the sol into a lyogel; c) optionally hydrophobization of the lyogel resulting in a hydrophobized lyogel; d) drying of the optionally hydrophobized lyogel so as to obtain an aerogel; said process being characterized in that the complete gelling step b) comprises dielectric heating by microwave or high-frequency electromagnetic irradiation, inducing an increase in temperature so as to reach a set temperature for complete gelling Tb in a range of from 100° C. to 200° C., preferably from 100° C. to 150° C., the temperature Tb being maintained in this range for a period of time U sufficient to attain complete gelling of the lyogel, and more particularly the end of syneresis of the lyogel.
申请公布号 FR3018207(B1) 申请公布日期 2016.03.18
申请号 FR20140051910 申请日期 2014.03.07
申请人 ENERSENS 发明人 BONNARDEL PIERRE-ANTOINE;CHAUSSON SOPHIE
分类号 B01J13/00 主分类号 B01J13/00
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