发明名称 |
METHOD FOR PRODUCING 2-OCTYL ACRYLATE BY DIRECT ESTERIFICATION |
摘要 |
The invention relates to a process for continuously producing 2-octyl acrylate by reacting acrylic acid and 2-octanol in the presence of a sulfonic acid esterification catalyst and at least one polymerization inhibitor. The water formed by the esterification reaction is entrained by distillation in a column surmounting the reactor in the form of a heteroazeotropic mixture with the 2-octanol which is then subjected, after condensation, to separation in a decanter so as to give an upper organic phase and a lower aqueous phase. The reaction mixture containing the reaction product and residual by-products are purified by separation means in order to obtain: (1) pure 2-octyl acrylate and (2) unreacted 2-octanol and acrylic acid compounds that will be recycled along with the catalyst. |
申请公布号 |
EP2773608(B1) |
申请公布日期 |
2015.10.21 |
申请号 |
EP20120794403 |
申请日期 |
2012.10.30 |
申请人 |
ARKEMA FRANCE |
发明人 |
RIONDEL, ALAIN;GRAIRE, CORALIE;LEVRAY, ANDRÉ;LINEMANN, REINHARD |
分类号 |
C07C67/08 |
主分类号 |
C07C67/08 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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