发明名称 |
METHOD OF MAKING A TEMPLATING AGENT |
摘要 |
A method for preparing 1-adamantyltrimethylammonium methylcarbonate or N,N-dimethyl-3,5-dimethylpiperidinium methylcarbonate is disclosed. The method comprises reacting dimethyl carbonate and 3,5-dimethylpiperidine or a 1-adamantylamine compound and in the presence of water in a sealed vessel at a temperature of from 80 to 200° C. The 1-adamantylamine compound is 1-adamantylamine, 1-adamantylmethylamine, or mixtures thereof. |
申请公布号 |
US2015065718(A1) |
申请公布日期 |
2015.03.05 |
申请号 |
US201414471737 |
申请日期 |
2014.08.28 |
申请人 |
JOHNSON MATTHEY PLC |
发明人 |
BRYAN RICHARD CHARLES |
分类号 |
C07D211/98;C07C68/06 |
主分类号 |
C07D211/98 |
代理机构 |
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代理人 |
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主权项 |
1. A method for preparing 1-adamantyltrimethylammonium methylcarbonate or N,N-dimethyl-3,5-dimethylpiperidinium methylcarbonate, comprising reacting dimethyl carbonate and 3,5-dimethylpiperidine or a 1-adamantylamine compound in the presence of water in a sealed vessel at a temperature of from 80 to 200° C., wherein the 1-adamantylamine compound is selected from the group consisting of 1-adamantylamine, 1-adamantylmethylamine, and mixtures thereof. |
地址 |
London GB |