| 发明名称 |
PROCESS FOR MANUFACTURING HMB AND SALTS THEREOF |
| 摘要 |
A continuous process and system for manufacturing beta-hydroxy-beta-methylbutyrate (HMB) and salts thereof is provided. The continuous process includes providing at least one oxidant and diacetone alcohol, and combining the at least one oxidant with the diacetone alcohol in a first flow reactor to produce a product stream comprising HMB or a salt thereof. Optionally, the process includes a second flow reactor for the acidification of a salt of beta-hydroxy-beta-methylbutyrate to produce beta-hydroxy-beta-methylbutyrate in free acid form. |
| 申请公布号 |
US2014256980(A1) |
申请公布日期 |
2014.09.11 |
| 申请号 |
US201214238802 |
申请日期 |
2012.08.15 |
| 申请人 |
Li Yao-En |
发明人 |
Li Yao-En |
| 分类号 |
C07C51/29 |
主分类号 |
C07C51/29 |
| 代理机构 |
|
代理人 |
|
| 主权项 |
1. A continuous process for manufacturing beta-hydroxy-beta-methylbutyrate or a salt thereof, comprising:
(A) providing at least one oxidant; (B) providing diacetone alcohol, wherein an equivalence ratio of the at least one oxidant to the diacetone alcohol is within a range of 3:1 to 4:1; and (C) combining the at least one oxidant with the diacetone alcohol in a flow reactor to form a product stream, wherein the temperature of the product stream is within a range of −10° C. to 40° C. |
| 地址 |
Buffalo Grove IL |
