发明名称 Fabrication Method Of Lithium Ceramics Pebbles Using Slurry Droplet Wetting Method
摘要 PURPOSE: A production method of a lithium ceramics pebble is provided to easily control a microstructure of the lithium ceramics pebble by controlling the sintering temperature and using a slurry droplet wet process. CONSTITUTION: A production method of a lithium ceramics pebble comprises the following steps: mixing lithium ceramics powder with a binder and deionized water mixture solution to obtain lithium ceramics slurry; dripping the lithium ceramics slurry in a hydroperoxide solution to obtain droplets; and drying and sintering the droplets. 7-20 wt% of binder is mixed in the binder and deionized water mixture solution. The concentration of the hydroperoxide solution is 5-40 wt%. The diameter of the droplets is 0.5-4.0 mm. The drying process is conducted at room temperature, and the sintering process is conducted at 600-1,300°C. [Reference numerals] (AA) Purified water; (BB) Li_4 SiO_4 powder; (CC) PVA solution (10 wt.%, 15 wt.%); (DD) Mix; (EE) Drop in hydroperoxide solution; (FF) Dry; (GG) Sinter (900°C, 950°C, 1000°C)
申请公布号 KR101328807(B1) 申请公布日期 2013.11.13
申请号 KR20120031248 申请日期 2012.03.27
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分类号 B01J2/02;C04B35/01;C04B35/622;C04B35/64 主分类号 B01J2/02
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