发明名称 5-ACETOXY-(E3)-3-PENTENYL-METHOXYMETHYLETHER AND PRODUCTION METHOD OF (E3)-3-ALKENYLACETATE USING THE SAME
摘要 PROBLEM TO BE SOLVED: To provide 5-acetoxy-(E3)-3-pentenyl-methoxymethylether producible in a common reaction installation; and a production method of (E3)-3-alkenylacetate using the same.SOLUTION: A 4-formyl-(E3)-3-butenyl-methoxymethylether is reacted with a reducing agent, and the obtained 5-hydroxy-(E3)-3-pentenyl-methoxymethylether is reacted with an acetylating agent to produce 5-acetoxy-(E3)-3-pentenyl-methoxymethylether. The 5-acetoxy-(E3)-3-pentenyl-methoxymethylether is subjected to coupling reaction with a Grignard reagent, and the obtained (E3)-3-alkenyl-methoxymethylether is treated with an acid, followed by reaction with an acetylating agent to produce (E3)-3-alkenylacetate.
申请公布号 JP2013189391(A) 申请公布日期 2013.09.26
申请号 JP20120055855 申请日期 2012.03.13
申请人 SHIN-ETSU CHEMICAL CO LTD 发明人 MIYAKE HIROKI;ISHIBASHI NAOKI;YAMASHITA MIYOSHI;FUKUMOTO TAKEHIKO
分类号 C07C69/145;C07B61/00;C07C67/08;C07C69/007 主分类号 C07C69/145
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