发明名称 |
METHOD OF PRODUCING POLYTHIOL COMPOUND FOR THIOEPOXY BASED OPTICAL MATERIAL, AND COPOLYMERIZABLE COMPOSITION FOR THIOEPOXY BASED OPTICAL MATERIAL COMPRISING THE POLYTHIOL COMPOUND |
摘要 |
PURPOSE: A manufacturing method of a polythiol compound is provided to manufacture a polythiol compound with low discoloration by controlling the calcium content in a thiourea which is for the synthesis of a polythiol compound for a thioepoxy-based optical material. CONSTITUTION: A manufacturing method of a bis(2-mercaptoethyl)sulfide for a thioepoxy-based optical material includes a step of obtaining a bis(2-hydroxyethyl)sulfide by the reaction of 2-chloroethanol and 2-mercaptoethanol; a step of obtaining a thiouronium by the reaction of a thiourea and the bis(2-hydroxyethyl)sulfide; and a step of obtaining a bis(2-mercaptoetyhl)sulfide by hydrolyzing the thiouronium. The calcium content in the thiourea is 1 wt% or less. |
申请公布号 |
KR20130086571(A) |
申请公布日期 |
2013.08.02 |
申请号 |
KR20130008476 |
申请日期 |
2013.01.25 |
申请人 |
KOC SOLUTION CO., LTD. |
发明人 |
JANG, DONG GYU;ROH, SOO GYUN;KIM, JONG HYO |
分类号 |
C07C319/02;C08G18/52;C08G18/58;G02B1/04 |
主分类号 |
C07C319/02 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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