发明名称 METHOD OF PRODUCING POLYTHIOL COMPOUND FOR THIOEPOXY BASED OPTICAL MATERIAL, AND COPOLYMERIZABLE COMPOSITION FOR THIOEPOXY BASED OPTICAL MATERIAL COMPRISING THE POLYTHIOL COMPOUND
摘要 PURPOSE: A manufacturing method of a polythiol compound is provided to manufacture a polythiol compound with low discoloration by controlling the calcium content in a thiourea which is for the synthesis of a polythiol compound for a thioepoxy-based optical material. CONSTITUTION: A manufacturing method of a bis(2-mercaptoethyl)sulfide for a thioepoxy-based optical material includes a step of obtaining a bis(2-hydroxyethyl)sulfide by the reaction of 2-chloroethanol and 2-mercaptoethanol; a step of obtaining a thiouronium by the reaction of a thiourea and the bis(2-hydroxyethyl)sulfide; and a step of obtaining a bis(2-mercaptoetyhl)sulfide by hydrolyzing the thiouronium. The calcium content in the thiourea is 1 wt% or less.
申请公布号 KR20130086571(A) 申请公布日期 2013.08.02
申请号 KR20130008476 申请日期 2013.01.25
申请人 KOC SOLUTION CO., LTD. 发明人 JANG, DONG GYU;ROH, SOO GYUN;KIM, JONG HYO
分类号 C07C319/02;C08G18/52;C08G18/58;G02B1/04 主分类号 C07C319/02
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