发明名称 |
METHOD FOR PRODUCING ZIRCONIUM TETRA CHLORIDE BY USING SILICON TETRA CHLORIDE |
摘要 |
PURPOSE: A manufacturing method of tetrachloride zirconium using silicon tetrachloride is provided to increase the productivity of zirconium tetrachloride with little amount of carbon by re-chloridizing zircon sand using plenty of silicon tetrachloride generated from a zircon chloridation process. CONSTITUTION: A manufacturing method of tetrachloride zirconium includes the steps of: obtaining a gaseous reaction product by generating a reaction between solid zircon sand, solid carbon, and chlorine gas based on equation 1, ZrSiO4 + 4C + 4Cl2 = ZrCl4 + SiCl4 + 4CO; and obtaining gaseous zirconium tetrachloride by generating a reaction between the gaseous reaction product and silicon tetrachloride based on equation 2, ZrSiO4 + SiCl4 = ZrCl4 + 2SiO2. The method further includes a step of cooling/coagulating zirconium tetrachloride based on the gaseous reaction product obtained from the reactions based on the equations. A manufacturing apparatus of tetrachloride zirconium includes a first reactor (4) and a second reactor (10).
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申请公布号 |
KR20130076194(A) |
申请公布日期 |
2013.07.08 |
申请号 |
KR20110144684 |
申请日期 |
2011.12.28 |
申请人 |
POSCO;RESEARCH INSTITUTE OF INDUSTRIAL SCIENCE & TECHNOLOGY |
发明人 |
LEE, CHANG KYU;CHOI, MI SEON;LEE, GO GI;JUNG, JAE YOUNG |
分类号 |
C01G25/04;B01D21/00;B01J8/32;B01J19/24 |
主分类号 |
C01G25/04 |
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