发明名称 METHOD OF PRODUCING 1,1,1,3-TETRAPHENYLPROPYNE
摘要 FIELD: chemistry.SUBSTANCE: invention relates to a method of producing 1,1,1,3-tetraphenylpropyne from a metal derivative of phenyl acetylene and triphenyl chloromethane in the medium of an organic solvent. The method is characterised by that the metal derivative of phenyl acetylene used is lithium tetraphenyl ethinyl alanate, and the organic solvent used is pure 1,4-dioxane. The reaction is carried out while heating at boiling point of the solvent for 1 hour.EFFECT: invention provides a method of producing 1,1,1,3-tetraphenylpropyne, which provides reproducible results with good output of the end product.1 cl, 1 ex
申请公布号 RU2473531(C1) 申请公布日期 2013.01.27
申请号 RU20110149507 申请日期 2011.12.05
申请人 FEDERAL'NOE GOSUDARSTVENNOE BJUDZHETNOE OBRAZOVATEL'NOE UCHREZHDENIE VYSSHEGO PROFESSIONAL'NOGO OBRAZOVANIJA "KUBANSKIJ GOSUDARSTVENNYJ UNIVERSITET" (FGBOU VPO "KUBGU") 发明人 KONSHIN VALERIJ VIKTOROVICH;TURMASOVA ANNA ALEKSEEVNA;KONSHINA DZHAMILJA NAIBOVNA
分类号 C07C15/50;C07C1/32;C07C11/22 主分类号 C07C15/50
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