发明名称 Bis-(1(2)H-tetrazol-5-yl) amine and production method therefor
摘要 High-quality bis-(1(2)H-tetrazol-5-yl)amine and a method for easily, safely, and inexpensively producing the compound are provided. The method for producing bis-(1(2)H-tetrazol-5-yl)amine includes the steps of heating to 50 to 120° C. a solution mixture in which a necessary amount of an azide salt and a dicyanamide salt in an amount corresponding to 1 to 80 wt % of a necessary amount are added to a solvent, adding an acid in an amount of 1.54 to 2.22 chemical equivalents of the dicyanamide salt in the solution mixture to carry out a reaction at 50 to 120° C., and then adding an acid and a dicyanamide salt solution in which the remaining dicyanamide salt is dissolved in a solvent to promote the reaction. Bis-(1(2)H-tetrazol-5-yl)amine is obtained according to the production method.
申请公布号 US8350050(B2) 申请公布日期 2013.01.08
申请号 US201113183064 申请日期 2011.07.14
申请人 TOYO BOSEKI KABUSHIKI KAISHA;TODA TOSHIYUKI;KOFUKUDA TORU 发明人 TODA TOSHIYUKI;KOFUKUDA TORU
分类号 C07D257/04 主分类号 C07D257/04
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