发明名称 METHOD OF PRODUCING 2,6-DIISOBORNYL-4-HYDROXY-4-METHYL-2,5-CYCLOHEXADIEN-1-ONE
摘要 FIELD: chemistry. ^ SUBSTANCE: invention relates to a method of producing 2,6-diisobornyl-4-hydroxy-4-methyl-2,5-cyclohexadien-1-one. The method involves oxidation of phenol in an organic solvent by bubbling an oxidant into a reaction mixture or adding an oxidant solution by drops in an organic solvent at temperature from -10 to 40C. The oxidant used is chlorine dioxide, the phenol used is terpenic phenol, specifically 2,6-diisobornyl-4-methylphenol in an organic solvent. The molar ratio of reactants is equal to 1:1-5, respectively. ^ EFFECT: invention increases output of 2,6-diisobornyl-4-hydroxy-4-methyl-2,5-cyclohexadien-1-one. ^ 10 cl, 15 ex
申请公布号 RU2458901(C1) 申请公布日期 2012.08.20
申请号 RU20110109627 申请日期 2011.03.14
申请人 UCHREZHDENIE ROSSIJSKOJ AKADEMII NAUK INSTITUT KHIMII KOMI NAUCHNOGO TSENTRA URAL'SKOGO OTDELENIJA RAN 发明人 LOGINOVA IRINA VALERIANOVNA;CHUKICHEVA IRINA JUR'EVNA;KUCHIN ALEKSANDR VASIL'EVICH
分类号 C07C13/23 主分类号 C07C13/23
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