发明名称 |
METHOD FOR PREPARING α,β-UNSATURATED ALDEHYDE |
摘要 |
PURPOSE: A manufacturing method of α,β-unsaturated aldehydes is provided to have few side reactions, to have excellent selectivity of products, and to manufacture α,β-unsaturated aldehydes efficiently and effectively. CONSTITUTION: A manufacturing method of α,β-unsaturated aldehydes comprises a step of aldol condensation reacting aldehyde and 0.2-2.0% NaOH aqueous solution at 90-130 °C. The weight ratio of the aldehyde and the NaOH aqueous solution is 1.0:0.6 - 1.0:1.7. The aldol condensation is symmetrical aldol condensation. The aldehyde is n aldehyde. The NaOH aqueous solution is 0.8-1.0 % NaOH aqueous solution. The aldol-condensation is conducted in 1-10 bar, by CSTR(continuous reactor).
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申请公布号 |
KR20120035368(A) |
申请公布日期 |
2012.04.16 |
申请号 |
KR20100096856 |
申请日期 |
2010.10.05 |
申请人 |
LG CHEM. LTD. |
发明人 |
KWON, O HARK;EOM, SUNG SHIK;KO, DONG HYUN;HONG, MOO HO;KIM, DAE CHUL;CHOI, JAE HUI |
分类号 |
C07C45/74;C07C47/21 |
主分类号 |
C07C45/74 |
代理机构 |
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主权项 |
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地址 |
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