摘要 |
A method for producing a polyarylene sulfide by reacting, in an organic polar solvent, a sulfidizing agent with a dihalogenated aromatic compound in the presence of an alkali metal hydroxide, which comprises: <step (1)> for conducting the reaction in such a manner that the polymerization time (T1a) within a temperature range of 230°C inclusive to 245°C exclusive is 30 minutes inclusive to 3.5 hours exclusive and, at the end point of the step, the conversion ratio of the dihalogenated aromatic compound is 70-98 mol%; and <step (2)> for conducting the reaction in such a manner that the polymerization time (T2) within a temperature range of 245°C inclusive to 280°C exclusive is 5 minutes inclusive to 1 hour exclusive. |
申请人 |
TORAY INDUSTRIES, INC.;UNOHARA, TAKESHI;ISAGO, HIROYUKI;NISHIMURA, TORU;INOHARA, MASAHIRO |
发明人 |
UNOHARA, TAKESHI;ISAGO, HIROYUKI;NISHIMURA, TORU;INOHARA, MASAHIRO |