发明名称 METHOD OF PURIFYING 1,2-PHENYLENEDIAMINE
摘要 FIELD: chemistry. ^ SUBSTANCE: invention relates to a novel improved method of purifying 1,2-phenylenediamine, involving distillation at normal pressure. During distillation, one of aliphatic alcohols - ethyl, propyl or isopropyl or their mixture in arbitrary ratio is put into the distillate receiving vessel and the obtained alcohol solution is cooled to 5-10C and 1,2-phenylenediamine is filtered. ^ EFFECT: method enables production of high-purity 1,2-phenylenediamine and its storage for a long period of time without change in colour. ^ 1 cl, 6 ex
申请公布号 RU2385860(C1) 申请公布日期 2010.04.10
申请号 RU20080142943 申请日期 2008.10.29
申请人 GOSUDARSTVENNOE UCHREZHDENIE MEDITSINSKIJ RADIOLOGICHESKIJ NAUCHNYJ TSENTR RAMN 发明人 DEEVA VALENTINA SEMENOVNA;DEEV VLADIMIR BORISOVICH;SKVORTSOV VALERIJ GRIGOR'EVICH
分类号 C07C209/84;C07C211/51 主分类号 C07C209/84
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