发明名称 METHOD OF PRODUCING TRIETHANOLAMINE
摘要 FIELD: chemistry. ^ SUBSTANCE: phosphoric and/or hypophosphorus acid and a basic compound are added to triethanolamine, where the basic compound is selected from a hydroxide of alkali metals, a hydroxide of alkali-earth metals and [R1R2R3(2-hydroxyethyl)ammonium]hydroxide, where R1, R2 and R3 independently denote an alkyl having 1-30 carbon atoms, or hydroxyalkyl having 2-10 carbon atoms. If a hydroxide of alkali metals is used as the basic compound, molar ratio of acid (acids): hydroxide ranges from 1:0.1 to 1:1, and if hydroxide of alkali-earth metals is used as the basic compound, molar ratio of acid (acids): hydroxide ranges from 1:0.05 to 1:0.5. Phosphoric and/or hypophosphorus acid and the basic compound are added before and/or during distillation of triethanolamine. The invention also relates to triethanolamine containing 0.01-2 wt % (in terms of pure triethanolamine) phosphoric and/or hypophosphorus acid and the corresponding hydroxide. ^ EFFECT: stability of improved chromaticity of triethanolamine during storage and increased output during distillation of the triethanolamine. ^ 15 cl, 2 tbl
申请公布号 RU2385315(C2) 申请公布日期 2010.03.27
申请号 RU20070111553 申请日期 2005.08.04
申请人 BASF AKTSIENGEZEL'SHAFT 发明人 KHEHZE FRANK;MEL'DER JOKHANN-PETER;DOSTALEK ROMAN;JULIUS MANFRED
分类号 C01B25/163;C01B25/165;C01D1/04;C07C213/10;C07C215/12;C07C215/40 主分类号 C01B25/163
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