发明名称 Method for producing barium titanium oxide single-crystal piece using containerless processing
摘要 Disclosed is a method for producing a barium titanium oxide single crystal piece with a given structure using a containerless solidification process, which comprises the steps of preparing a material made of a barium titanium oxide, controlling the material to be in a levitated state within a levitation furnace, melting the levitated material using a laser, and solidifying the molten material while maintaining the levitated state. In a specific embodiment, a spherical sample having a composition of BaTiO3 and a weight of about 20 mg is subjected to a rapid solidification and melting process (temperature gradient: about 700 K/sec) 3 times while levitating the sample in 4.5 atm of air atmosphere using an electrostatic levitation furnace. Then, the re-molten sample is maintained at a temperature just below the melting point of the sample for a given time, and then rapidly cooled at a cooling rate of 300 K/sec to obtain a transparent blue barium titanium oxide single crystal. The single crystal exhibits innovative dielectric characteristics having a large relative permittivity (100,000 or more at room temperature) and a low dielectric loss. In addition, the single crystal has excellent temperature stability allowing the relative permittivity to be gently reduced in the range of room temperature to 70 K.
申请公布号 US7544245(B2) 申请公布日期 2009.06.09
申请号 US20050044325 申请日期 2005.01.28
申请人 JAPAN AEROSPACE EXPLORATION AGENCY 发明人 YONO KENTEI;PARADIS PAUL-FRANCOIS;ISHIKAWA TAKEHIKO;YODA SHINICHI
分类号 C30B29/32;C30B30/00;C04B35/46;C04B35/48;C04B35/49;C30B1/00;C30B13/00;C30B30/04;C30B30/08 主分类号 C30B29/32
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