发明名称 METHOD FOR CONTINUOUS PRODUCTION OF 9,9-BIS(4-HYDROXYPHENYL)FLUORENES BY USING CLATHRATE CRYSTAL
摘要 PROBLEM TO BE SOLVED: To obtain a high-quality product by making the production process continuous. SOLUTION: The production process contains a reaction step to form a 9,9-bis(4-hydroxyphenyl)fluorenes, a dehydration step to dehydrate the reaction product obtained by the reaction step, a concentration step to concentrate the 9,9-bis(4-hydroxyphenyl)fluorenes, a crystallization step to crystallize a clathrate compound from a mixture of a solvent and the concentrated liquid, a crystallized product separation step to separate the slurry, the mother liquor and the washing liquid, a solvent removing step to remove the solvent from the slurry containing the clathrate compound obtained by the crystallized product separation step, a solvent purifying step to purify at least a part of the liquid containing the solvent obtained by the solvent removing step, the mother liquor obtained by the crystallized product separation step and the washing liquid, and a phenols purifying step to purify at least a part of the liquid obtained by the solvent purifying step. COPYRIGHT: (C)2008,JPO&INPIT
申请公布号 JP2008115139(A) 申请公布日期 2008.05.22
申请号 JP20060302416 申请日期 2006.11.08
申请人 OSAKA GAS CO LTD;TSUKISHIMA KIKAI CO LTD 发明人 MURASE HIROAKI;OGATA KAZUYUKI;MIYAUCHI SHINSUKE;SUDA HIDEKI;KANBE TATSUYA;FUKADA MITSURU;OKADA AKIHISA
分类号 C07C37/20;C07B61/00;C07C39/17 主分类号 C07C37/20
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