摘要 |
<p>[Problem] In known methods, an improvement of the coercive force is realized by allowing the Dy metal or the like to present selectively in crystal grain boundary portions of a sintered magnet. However, since these are based on a physical film formation method, e.g., sputtering, through the use of a vacuum vessel, there is a mass productivity problem in the case where large amounts of magnet is treated. Furthermore, there is a magnet cost problem from the viewpoint that, for example, an expensive, high-purity Dy metal or the like must be used as a raw material for film formation. [Solving Means] A method for modifying grain boundaries of a Nd-Fe-B base magnet characterized by including the step of allowing an M metal component to diffuse and penetrate from a surface of a Nd-Fe-B base sintered magnet body having a Nd-rich crystal grain boundary phase surrounding principal Nd 2 Fe 14 B crystals to the grain boundary phase through a reduction treatment of a fluoride, an oxide, or a chloride of an M metal element (where M is Pr, Dy, Tb, or Ho).</p> |