发明名称 |
A PROCESS FOR THE PREPARATION OF 1-MONO (C1-C4)ALKYLNAPHTALENE |
摘要 |
The invention concerns a process for the preparation of 1-mono(C1-C4) alkyl naphthalene, which consists in that an interaction of alcohol is performed with alkyl chain C1-C4 with naphthalene and polyphosphoric acid in the presence of n-toluene sulfonic acid as catalyst at heating, at that alcohol is used at 1.5 fold excess and into the synthesis there is introduced for 2.5-3 hours with maintainingtemperature of 75-85 DEGREE C, and the obtained reaction mass is kept in these conditions for not less than 1 hour to a complete finishing the reaction.
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申请公布号 |
UA78660(C2) |
申请公布日期 |
2007.04.10 |
申请号 |
UA20060004922 |
申请日期 |
2006.05.03 |
申请人 |
INSTITUTE OF SCINTILLATION MATERIALS OF THE NATIONAL ACADEMY OF SCIENCES OF UKRAINE |
发明人 |
HRYNIOV BORYS VIKTOROVYCH;BEDRYK OLEKSANDRA IVANIVNA;SHERSHUKOV VIKTOR MYKHAILOVYCH |
分类号 |
C07C2/00;C07C15/24 |
主分类号 |
C07C2/00 |
代理机构 |
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