METHOD FOR PRODUCTION OF COPPER (II) AND ZINC (II) ACETYLACETONATES

摘要

FIELD: production of high temperature superconductors. ^ SUBSTANCE: invention relates to electrochemical synthesis of metal beta-diketonates, in particular acetylacetonates. Synthesis of Cu(II) and Zn(II) acetylacetonates in carried out by electrolysis of acetylacetone solution and base electrolyte in acetonitryl in ratio of (1:10):0.5:100, with electrodes made of metal presenting in produced acetylacetonate, at current density not more mA/cm2 by using pulse current. Pulse time is controlled by pulse forming unit connected in parallel to elecrtolyzer. As base electrolyte preferably lithium perchlorate or lithium chloride is used. ^ EFFECT: controlled process for production of metal acetylacetonates. ^ 5 cl, 2 ex, 1 dwg