发明名称 METHOD FOR PREPARING MIXTURES OF POLYALKYLADAMANTANES
摘要 FIELD: organic chemistry, chemical technology. ^ SUBSTANCE: method involves the alkylation reaction of adamantine or mixture of alkyladamantanes with the general number of carbon atoms 11-20 in methylene chloride solution medium at temperature 15-25°C in the presence of catalytic system representing an equimolar mixture of aluminum halide and halide-containing promoter of the general formula: AlX3 x CpHrXz wherein X means Cl, Br; p = 0; r = 0; z = 2, or P = 1; z = 4, either p = 1; r = 2; z = 2. The conversion of adamantine is 78-94%. Invention provides the development of the improved technological procedure for preparing the end substances with the enhanced importance. ^ EFFECT: improved preparing method. ^ 7 tbl, 16 ex
申请公布号 RU2277080(C1) 申请公布日期 2006.05.27
申请号 RU20050102495 申请日期 2005.02.02
申请人 发明人 AKHREM IRENA SERGEEVNA;AFANAS'EVA LJUDMILA VJACHESLAVOVNA;VITT SERGEJ VLADIMIROVICH;CHURILOVA IRINA MIKHAJLOVNA;NESMELOV ALEKSANDR IGOREVICH;DULOVA VERA GRIGOR'EVNA
分类号 C07C13/615;C07C2/66 主分类号 C07C13/615
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