发明名称 |
PROCESS FOR PURIFYING STERICALLY HINDERED 4-AMINO PIPERIDINES |
摘要 |
A process for purifying raw piperidines of formula (I), where R1 to R4 are C 1 to C6 alkyl, R1 and R2 and/or R3 and R4 together are a CH2 chain with 2 to 5 C atoms. Said process is characterized in that in an initial step high-boiling-point substances and possible water are eliminated by distillation from the raw piperidines, in a second step 0.01 to 5 wt %, in relation to the product of the first step, of a reducing agent are add ed and in a third step the piperidines are isolated by distillation.
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申请公布号 |
CA2257095(C) |
申请公布日期 |
2005.02.01 |
申请号 |
CA19972257095 |
申请日期 |
1997.05.30 |
申请人 |
BASF AKTIENGESELLSCHAFT |
发明人 |
RUST, HARALD;KRAUSE, ALFRED;JULIUS, MANFRED;SIEGEL, HARDO;WITZEL, TOM;SIEGEL, WOLFGANG |
分类号 |
C07D211/58;C07D211/56;(IPC1-7):C07D211/58;C07D221/20 |
主分类号 |
C07D211/58 |
代理机构 |
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