发明名称 |
Process for the preparation of aqueous sodium methioninate solutions and use of these solutions for the preparation of a granulate |
摘要 |
<p>Production of aqueous sodium methioninate (I) solution containing little sodium carbonate from the crude mixture from alkaline hydrolysis of 5-( beta -methylmercapto-ethyl)-hydantoin (II) comprises: (a) distilling water from mixture, preferably with sodium hydroxide addition, until the (I) content is 60-90 wt.%; and (b) separating the sodium carbonate precipitate at 90-140 degrees C. Production of aqueous sodium methioninate (I) solution containing little sodium carbonate from the crude mixture from the alkaline hydrolysis of 5-( beta -methylmercapto-ethyl)-hydantoin (II) with 1.1-6 equivalents of sodium hydroxide and/or carbonate comprises: (a) distilling water from the mixture, preferably with addition of more sodium hydroxide, until the (I) content is 60-90 wt.%; and (b) separating the sodium carbonate precipitate in anhydrous form or as monohydrate and/or bicarbonate, at 90-140 degrees C. An Independent claim is also included for free-running (I) granulate.</p> |
申请公布号 |
EP0959068(B1) |
申请公布日期 |
2004.12.15 |
申请号 |
EP19990108788 |
申请日期 |
1999.05.03 |
申请人 |
DEGUSSA AG |
发明人 |
KOERFER, MARTIN;ROHLAND, LUTZ;BINDER, WOLFRAM DR.;HASSELBACH, HANS JOACHIM DR.;ALT, HANS CHRISTIAN;HUTHMACHER, KLAUS DR.;KNIESEL, HEIDEMARIE DR. |
分类号 |
A23K1/16;A23K1/22;C07C319/20;C07C319/28;C07C323/58;(IPC1-7):C07C319/20;C07C323/60 |
主分类号 |
A23K1/16 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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