发明名称 Method for production of alkoxylated compound
摘要 When the reaction solution formed during the addition of an alkylene oxide to an active hydrogen-containing compound has viscosity of not less than 10 mPa.s, this invention provides a method for stirring the reaction solution by the rotation of a vane or vanes continuously disposed in the vertical direction within an agitating reaction vessel in such a manner that the numerical value C represented by the following formula (1):(wherein A denotes the length (m) of the vane or the vanes newly immersed by the supply of alkylene oxide, h1 denotes the height (m) of the liquid level before the supply of alkylene oxide, and h2 denotes the height (m) of the liquid level after the supply of alkylene oxide) may be not less than 0.5. By employing the method of this invention, it is made possible to effect addition of an alkylene oxide to the active hydrogen-containing compound with high efficiency. Further, the use of this method allows repression of the content of a by-product which causes the degradation of the characteristic properties of the alkoxylated compound.
申请公布号 US6762325(B2) 申请公布日期 2004.07.13
申请号 US20020144491 申请日期 2002.05.13
申请人 NIPPON SHOKUBAI CO., LTD. 发明人 INAOKA TORU;SATO YASUHIKO;ONDA YOSHIYUKI;TANAKA HIROMICHI;HIRATA TSUYOSHI
分类号 B01F7/18;B01J10/00;B01J19/00;B01J19/18;C04B24/26;C04B24/32;C08G65/26;(IPC1-7):C07C213/00;C07C41/03 主分类号 B01F7/18
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