发明名称 METHOD FOR PREPARING alpha,alpha-DIMETHYLPHENYLACETIC ACID FROM alpha,alpha-DIMETHYLBENZYLCYANIDE WITHOUT PRESSURE
摘要 FIELD: organic chemistry, chemical technology. SUBSTANCE: invention relates to the improved method for preparing alpha,alpha--dimethylphenylacetic acid without using the enhanced pressure wherein alpha,alpha-dimethylbenzylcyanide is converted to the corresponding carboxylic acid salt in the presence of water, sodium hydroxide and C4-alcohol and/or C5-alcohol at temperature above 100 C followed by preparing alpha,alpha-dimethylphenylacetic acid by addition of acid. Method provides preparing the impurity-free end product with high yield 97.3%. EFFECT: improved preparing method, enhanced yield. 8 cl, 2 ex
申请公布号 RU2227137(C2) 申请公布日期 2004.04.20
申请号 RU20010111316 申请日期 1999.09.15
申请人 发明人 KORB GERKHARD;FLEMMING KHANS-VOL'FRAM;LENERT RUDOL'F;RYBCHINSKI VOL'FGANG
分类号 C07C51/08;C07C57/30 主分类号 C07C51/08
代理机构 代理人
主权项
地址