发明名称 |
PROCESSES FOR THE PURIFICATION OF BIS(2-HYDROXYETHYL) TEREPHTHALATE |
摘要 |
The invention aims at providing a process for recovering high-purity bis(2-hydroxylethyl) terephthalate (BHET) efficiently from an ethylene glycol (EG) solution containing crude BHET, particularly a depolymerization solution obtained by depolymerizing a polyester comprising polyethylene terephthalate (PET) as the main component with EG, while suppressing the formation of impurities such as diethylene glycol (DEG), DEG esters and oligomers. The invention relates to a process for the purification of BHET which comprises crystallizing the depolymerization solution under specified temperature conditions and subjecting the obtained mixture to solid-liquid separation, and to a process for the purification of BHET which comprises the evaporation step of evaporating low-boiling components from the depolymerization solution under specified conditions to thereby obtain a melt and the molecular distillation step of distilling the obtained melt under specified conditions and recovering a specific fraction.
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申请公布号 |
WO03101929(A1) |
申请公布日期 |
2003.12.11 |
申请号 |
WO2003JP06878 |
申请日期 |
2003.05.30 |
申请人 |
AIES CO., LTD.;INADA, SHUJI;SATO, KIKUCHI |
发明人 |
INADA, SHUJI;SATO, KIKUCHI |
分类号 |
C07C67/52;C07C67/54;(IPC1-7):C07C69/82;C07C67/03;C08J11/24 |
主分类号 |
C07C67/52 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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