发明名称 Process for production of polyamide
摘要 In the process for producing polyamide of the present invention, a diamine and a dicarboxylic acid are melt-polycondensed in a batch-wise fist polymerizer in the absence of a solvent to produce a middle-stage polyamide. The diamine has a boiling point higher than a melting point of the middle-stage polyamide being produced under inner pressures of the first polymerizer. The middle-stage polyamide is fed into a continuous second polymerizer while controlling the change of relative viscosity within ±0.2, and further polycondensed there to produce the objective polyamide. With such a process, the change of polymerization degree of the middle-stage polyamide during the switching of the polymerization step from a batch-wise manner to a continuous manner is avoided, thereby preventing the variation in quality of the final product.
申请公布号 US6657037(B2) 申请公布日期 2003.12.02
申请号 US20020038587 申请日期 2002.01.08
申请人 MITSUBISHI GAS CHEMICAL COMPANY, INC. 发明人 TANAKA KAZUMI;SHIDA TAKATOSHI;KUROSE HIDEYUKI
分类号 C08G69/30;C08G69/04;C08G69/28;(IPC1-7):C08G69/02;C08G69/06 主分类号 C08G69/30
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