发明名称 |
PROCESS FOR PRODUCING N,N-DISUBSTITUTED AMINOPHENOL |
摘要 |
A process for producing N,N-disubstituted aminophenol which comprises the steps of: obtaining a reaction mixture containing N-substituted aminophenol by reacting a dihydric phenol and an amine; subjecting said reaction mixture to heat treatment so as to thermally decompose quaternary ammonia salt contained in said reaction mixture into a dihydric phenol and an amine, and removing at least said amine by distillation; separating high-boiling impurities by distillation to separate N-substituted aminophenol; and subjecting said separated N-substituted aminophenol to reduction alkylation using an aldehyde compound. According to the present invention, high-purity N,N- disubstituted aminophenol can be obtained in a high yield at high selectivity, and a reduction catalyst can be used repeatedly because its activity can be maintained at a high level and yet it can retain high activity for a long period of time.
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申请公布号 |
CA2136102(C) |
申请公布日期 |
2003.12.02 |
申请号 |
CA19942136102 |
申请日期 |
1994.03.17 |
申请人 |
MITSUI PETROCHEMICAL INDUSTRIES LTD. |
发明人 |
NAGAMATSU, SHIGEKI;ARASE, TOMOHIRO;YASUDA, MASAAKI |
分类号 |
B01J23/40;B01J23/74;C07B61/00;C07C213/02;C07C213/08;C07C213/10;C07C215/76;(IPC1-7):C07C215/76 |
主分类号 |
B01J23/40 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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